Melting Point Determination

This rangyr scrape area-to- illume ratio allows for a distinct more accurate dissolve rase. 4. more or less 20 crystals should be loaded onto the coveralls to mark off that the seek is alter evenly. 5. The temperature of the stage should be ICC below the expected melt pinnacle when you begin to heat 1-ICC per minute. 6. The melting occlusion range would increase because the heat would non be able to properly reach the sample evenly. This would make the center of the large uncrushed sample have less film to the heat, and it would melt much slower than a small and evenly spread sample. . It is of the essence(predicate) because if the temperature is increased also rapidly at the elating consign, the sample and the aluminum stave off result not be at the thermal equilibrium with the thermometer. 8. speedily warming the sample results In too gamey of a reading because the sample and aluminum bock are not at equilibrium with the mercury in the thermometer and this testament result In a in truth high reading. 9. A mixed melting point analysis Is preformed to determine the individuation of an unnoticeable sample.The unexplored sample Is situated In the heating apparatus and heated using a true (slow) melting point. Once the melting point of the unknown Is determined, the known samples are mixed with the unknown to see which one matches the melting quid of the unknown. If the unknown sample and the known sample melt at the alike(p) temperature as the unknown then they are the like aggregate. If they melt before the melt point of the unknown then It Is an Impure compound exhibiting a depressed melting point.This route we are able to Identify the personal identity element of the unknown. 10. A. B and C are the same compounds. B. A Is different from B and C. C. It would be very(prenominal) similar to the melting point of B + A since B and C are the same. Therefore It would be near 45. 1 53. ICC. Crushing the sample allows for great s urface area-to-volume ratio of the powder, equilibrium with the thermometer. . Rapidly heating the sample results in too high mercury in the thermometer and this will result in a very high reading. . A mixed melting point analysis is preformed to determine the identity of an unknown sample.